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Making big particles to powder


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#1 NUKE

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Posted 11 February 2009 - 07:50 PM

Hello there.I have some barium nitrate which has formed something like rocks,if you can understand me, and i want to milled it in order to make it fine powder.So i put it in my ball mill,of course in an new jar with some lead balls.What i noticed is that the colour of barium nitrate changed from pure white to grey and this happens because lead is contaminating it.

And i want to know if that is as dangerous as i think and what else can i do in order to make it be fine powder.Thanks

#2 MDH

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Posted 11 February 2009 - 08:04 PM

I believe Lead Dioxide is sometimes used as a catalyst but otherwise I can't see how it'd dramatically increase the sensetivity of any composition. Poison should not be a concern, barium is already quite poisonous.

You may want to try a simple $10 coffee grinder. I use those to grind nitrates before I make any composition with them.

It's bizzare that your barium nitrate has formed rocks though. I've never had that problem before.

#3 digger

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Posted 11 February 2009 - 09:21 PM

I have had the problem of very finely milled Barium Nitrate forming one very solid lump that needed smashing with a hammer. It would pass through a sieve if grated against it, but it was difficult, much easier to chuck it in the mill for a while.

Although I have not had this problem with the coarser grades of Barium Nitrate.
Phew that was close.

#4 NUKE

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Posted 11 February 2009 - 10:57 PM

Actually i bought it this way,like a rock....Arggg...

Coffe griner,mmm,yes i will try that...

Thanks for your replies

#5 Mumbles

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Posted 13 February 2009 - 12:28 AM

It's pretty common for Ba(NO3)2 that has been sitting in a warehouse for a few years. Mine was the same way mostly. I just grate it against a relatively coarse screen to break it up as I use it. Sr(NO3)2 is the same way. Most fine powders will do this actually. I've had a drum, seriously that was one solid cake of Mg. I had to break it all up with an ice pick.




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